HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
(2-Methoxypyridin-4-yl)methanamine → 4-(Aminomethyl)pyridin-2(1H)-one
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | (2-Methoxypyridin-4-yl)methanamine | HCID 16227983 | — |
| Lösungsmittel | Hydrochloric Acid | HCID 313 | — |
| Produkt | 4-(Aminomethyl)pyridin-2(1H)-one | HCID 15079301 | — |
Reaktionsschritte
The starting material (2-methoxypyridin-4-yl)methanamine 56-2 in 3N HCl was refluxed at 110° C. for 12 hours. The reaction was taken to dryness by rotary evaporation to give crude 4-(aminomethyl)pyridin-2(1H)-one 56-3.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US09181235B2 |
| Quelldatensatz | uspto-grants-2015_11 |
| ORD ID | ord-0a0113fcf18d4c1b932891df2d2f6d59 |
| Quellennotiz | uspto-grants-2015_11 |