HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Benzoylhydrazine → N-(4-(2-(2-phenylacetyl)hydrazinecarbonyl)pyridin-2-yl)benzamide
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Benzoylhydrazine | HCID 11955 | — |
| Edukt | Benzeneacetic acid, hydrazide | HCID 70301 | — |
| Edukt | HCID 64393851 | HCID 64393851 | — |
| Produkt | N-(4-(2-(2-phenylacetyl)hydrazinecarbonyl)pyridin-2-yl)benzamide | HCID 67153966 | 65% |
Reaktionsschritte
Following the procedure as described in Preparation 13, making variations as required to replace benzohydrazide with 2-phenylacetohydrazide to react with 2-benzamidoisonicotinic acid, N-(4-(2-(2-phenylacetyl)hydrazinecarbonyl)pyridin-2-yl)benzamide was obtained in 65% yield: MS (ES+) m/z 374.9 (M+1).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US09187426B2 |
| Quelldatensatz | uspto-grants-2015_11 |
| ORD ID | ord-041b11ff412e435fbd512076e40afaa5 |
| Quellennotiz | uspto-grants-2015_11 |