HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
2H-1,4-benzoxazin-3(4H)-one → 6-(6-Bromohexanoyl)-2H-1,4-benzoxazin-3(4H)-one
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 2H-1,4-benzoxazin-3(4H)-one | HCID 72757 | — |
| Edukt | 6-Bromohexanoyl chloride | HCID 89848 | — |
| Produkt | 6-(6-Bromohexanoyl)-2H-1,4-benzoxazin-3(4H)-one | HCID 21886993 | 45,1% |
Reaktionsschritte
Using 2H-1,4-benzoxazin-3(4H)-one (15.0 g) and 6-bromohexanoyl chloride (25.8 g) according to the same method as that of Reference Example 1, the title compound (14.8 g) was obtained as colorless crystals.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07132547B2 |
| Quelldatensatz | uspto-grants-2006_11 |
| ORD ID | ord-f8799234a80d499aad3e610668af8ffd |
| Quellennotiz | uspto-grants-2006_11 |