HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 733288Erstellt: 24. Oktober 2026
2,2,3,3,3-Pentafluoropropanol → 2,2,3,3,3-Pentafluoropropyl trifluoromethanesulfonate
https://huagongshe.com/de/reaction/733288
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|
| Edukt | 2,2,3,3,3-Pentafluoropropanol | HCID 9872 | — |
| Edukt | Trifluoromethanesulfonic anhydride | HCID 67749 | — |
| Produkt | 2,2,3,3,3-Pentafluoropropyl trifluoromethanesulfonate | HCID 2776019 | 97% |
Reaktionsschritte
A mixture of trifluoromethanesulfonic anhydride (40 mL, 0.24 mol) and 2,2,3,3,3-pentafluoropropanol (25 mL, 0.24 mol) was heated under argon at 90° C. overnight. Then, the crude mixture was distilled at atmospheric pressure to give the desired product as a colourless oil (97% yield).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patentnummer | US07589125B2 |
|---|
| Quelldatensatz | uspto-grants-2009_09 |
|---|
| ORD ID | ord-5c7fcfdc30414347a5f208e1333ccbe4 |
|---|
| Quellennotiz | uspto-grants-2009_09 |
|---|
