HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Benzoyl chloride, 4-(hexyloxy)- → Ethyl[benzyl(4-{[4-(hexyloxy)benzoyl]amino}benzyl)amino]-(oxo)acetate
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Benzoyl chloride, 4-(hexyloxy)- | HCID 170235 | — |
| Edukt | Ethyl[(4-aminobenzyl)(benzyl)amino](oxo)acetate | HCID 67187687 | — |
| Produkt | Ethyl[benzyl(4-{[4-(hexyloxy)benzoyl]amino}benzyl)amino]-(oxo)acetate | HCID 67186531 | 58% |
Reaktionsschritte
The same procedure as employed in the preparation of Example 15, step d but using 4-hexyloxy-benzoyl chloride and ethyl[(4-aminobenzyl)(benzyl)amino](oxo)acetate gave the title compound as a colorless oil (58%). M−(ESI): 515.2. HPLC (Condition A), Rt: 6.0 min (HPLC purity: 94.9%).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07592477B2 |
| Quelldatensatz | uspto-grants-2009_09 |
| ORD ID | ord-e526092712d24841b39530a47b3d5632 |
| Quellennotiz | uspto-grants-2009_09 |