HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
p-Anisoyl chloride → Methyl 1-(4-methoxybenzamido)cyclohexane-1-carboxylate
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | p-Anisoyl chloride | HCID 7477 | — |
| Edukt | Methyl 1-aminocyclohexane-1-carboxylate hydrochloride | HCID 22645079 | — |
| Produkt | Methyl 1-(4-methoxybenzamido)cyclohexane-1-carboxylate | HCID 32468563 | 71% |
Reaktionsschritte
581 mg (3 mmol) of 1-aminocyclohexanecarboxylic acid methyl ester hydrochloride was used instead of 1-aminocyclohexanecarboxylic acid phenylmethyl ester, and 512 mg (3 mmol) of 4-methoxybenzoyl chloride was used instead of phenylacetyl chloride in the process according to Reference Example 1 to obtain 619 mg (71%) of the title compound.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US08829209B2 |
| Quelldatensatz | uspto-grants-2014_09 |
| ORD ID | ord-2dde8241bbcb427b9a110f37403ccdef |
| Quellennotiz | uspto-grants-2014_09 |