HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Ammonia → 1H-Isoindole-1,3(2H)-dione, hexahydro-
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Ammonia | HCID 222 | — |
| Edukt | Hexahydrophthalic anhydride | HCID 85689 | — |
| Produkt | 1H-Isoindole-1,3(2H)-dione, hexahydro- | HCID 73559 | — |
Reaktionsschritte
A mixture of 1,2-cyclohexanedicarboxylic anhydride (3 g; 19.5 mmol) and 29% aqueous ammonia (3.4 g) was heated and kept at an inner temperature of 180°-190° C. for 2 hours to give cyclohexane-1,2-dicarboximide. M.P. 132°-136° C.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04598078 |
| Quelldatensatz | uspto-grants-1986_07 |
| ORD ID | ord-2eaf246c17244b308780dd9329257100 |
| Quellennotiz | uspto-grants-1986_07 |