HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Diethylformamide → 6-Diethylamino-3,8-di-(pyrrolidinomethyleneamino)-phenanthridine
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Diethylformamide | HCID 12051 | — |
| Edukt | 1-Pyrrolidinecarboxaldehyde | HCID 77372 | — |
| Edukt | 3,8-Diamino-6-diethylaminophenanthridine | HCID 23314007 | — |
| Produkt | 6-Diethylamino-3,8-di-(pyrrolidinomethyleneamino)-phenanthridine | HCID 13345880 | 66% |
Reaktionsschritte
As in Example 14, but using 3,8-diamino-6-diethylaminophenanthridine and N-formylpyrrolidine instead of 3,8-diamino-6-dimethylaminophenanthridine and N,N-diethylformamide. Yield 66%, melting point 149°-150° C. (chloroform/petroleum ether (60°-80° C.)).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04599409 |
| Quelldatensatz | uspto-grants-1986_07 |
| ORD ID | ord-97ac297e36e14eefa5a32fef4f37b4e5 |
| Quellennotiz | uspto-grants-1986_07 |