HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
N,N,N',N'-Tetramethylazodicarboxamide → HCID 68821972, Verbindung
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | N,N,N',N'-Tetramethylazodicarboxamide | HCID 4278 | — |
| Edukt | Tributylphosphine | HCID 13831 | — |
| Edukt | ethyl (4-hydroxy-1H-indol-1-yl)acetate | HCID 68822476 | — |
| Edukt | 4-Pentyn-1-ol, 5-[4-(trifluoromethoxy)phenyl]- | HCID 68822690 | — |
| Produkt | HCID 68821972 | HCID 68821972 | — |
Reaktionsschritte
In analogy to the procedure described for example 1 d], (4-hydroxy-indol-1-yl)-acetic acid ethyl ester was reacted with 5-(4-trifluoromethoxy-phenyl)-pent-4-yn-1-ol in the presence of N,N,N′,N′-tetramethyl azodicarboxamide and tributylphosphine to give the title compound as colorless crystals.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07405236B2 |
| Quelldatensatz | uspto-grants-2008_07 |
| ORD ID | ord-8ce05be325b04819ac74769e7fc0d2aa |
| Quellennotiz | uspto-grants-2008_07 |