HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Acetaldehyde → HCID 178419035, Verbindung
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Acetaldehyde | HCID 177 | — |
| Edukt | Acetyl chloride | HCID 6367 | — |
| Edukt | 1,1,3,3-Tetramethylbutyl isocyanide | HCID 26725 | — |
| Edukt | 2-Amino-3-benzyloxypyridine | HCID 90334 | — |
| Lösungsmittel | Perchloric Acid | HCID 24247 | — |
| Produkt | HCID 178419035 | HCID 178419035 | — |
Reaktionsschritte
Example 9 was carried out in accordance with the general directions for synthesis in process step a) from 1.0 ml (0.1 mmol) 2-amino-3-benzyloxypyridine (0.1 M, DCM), 0.575 ml (0.115 mmol) 1,1,3,3-tetramethylbutylisonitrile solution (0.2 M, DCM), 0.500 ml (0.15 mmol) acetaldehyde solution (0.3 M, DCM) and 10 μl perchloric acid (w=20%) and in process step c) and d) by reacting the resultant reaction product with 0.4 mmol acetylchloride.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07087607B2 |
| Quelldatensatz | uspto-grants-2006_08 |
| ORD ID | ord-35de8171a48847fc924677310cf7789a |
| Quellennotiz | uspto-grants-2006_08 |