HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 78756Erstellt: 23. Oktober 2026
Potassium Carbonate → (3R,3aS,6aR)-hexahydrofuro(2,3-b)furan-3-ol
https://huagongshe.com/de/reaction/78756
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|
| Edukt | Potassium Carbonate | HCID 11430 | — |
| Edukt | (3R,3aS,6aR)-Hexahydrofuro[2,3-b]furan-3-yl acetate | HCID 59959307 | — |
| Lösungsmittel | Methanol | HCID 887 | — |
| Lösungsmittel | Dichloromethane | HCID 6344 | — |
| Produkt | (3R,3aS,6aR)-hexahydrofuro(2,3-b)furan-3-ol | HCID 9942150 | — |
Reaktionsschritte
(3R,3aS,6aR)-Hexahydrofuro[2,3-b]furan-3-yl acetate (8.0 g) was dissolved in dichloromethane (24 ml) and Methanol (24 ml). Potassium carbonate (0.1 g) was added and reaction mass was stirred at 25-35° C. till the completion of reaction. Reaction mass was filtered & concentrated under vacuum at 40-45° C. to residue of (3R,3aS,6aR)-Hexahydrofuro[2,3-b]furan-3-ol (Yield 6.5 g).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patentnummer | US08841467B2 |
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| Quelldatensatz | uspto-grants-2014_09 |
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| ORD ID | ord-7fb413531e564110ada8de0058b82c76 |
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| Quellennotiz | uspto-grants-2014_09 |
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