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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 80320Erstellt: 24. Oktober 2026

Iodoethane → Ethyl(triphenylmethyl)amine

https://huagongshe.com/de/reaction/80320

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktIodoethaneHCID 6340—
EduktTritylamineHCID 138598—
LösungsmittelAcetonitrileHCID 6342—
ProduktEthyl(triphenylmethyl)amineHCID 444736028%

Reaktionsschritte

Triphenylmethylamine (1.00 g, 3.86 mmol) (Wako Pure Chemical Industries, Ltd.) and iodoethane (1.50 g, 9.62 mmol) (Wako Pure Chemical Industries, Ltd.) were dissolved in acetonitrile (5 mL) (Wako Pure Chemical Industries, Ltd.), and the mixture was left to stand still at room temperature for 3 days. The solvent was distilled off under reduced pressure, and the residue was subjected to silica gel column chromatography (chloroform (Wako Pure Chemical Industries, Ltd.) as an eluent), to thereby obtain the title compound (0.31 g, 28% yield).

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS08846012B2
Quelldatensatzuspto-grants-2014_09
ORD IDord-b13daa3783284fc5acaee76552dcdb91
Quellennotizuspto-grants-2014_09