HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
3,4-Dimethoxybenzenesulfonyl chloride → 1-[(3,4-Dimethoxyphenyl)sulfonyl]-4-(1-piperazinyl)-1H-indole Hydrochloride
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 3,4-Dimethoxybenzenesulfonyl chloride | HCID 2734183 | — |
| Edukt | tert-Butyl 4-(1H-indol-4-yl)piperazine-1-carboxylate | HCID 22015386 | — |
| Produkt | 1-[(3,4-Dimethoxyphenyl)sulfonyl]-4-(1-piperazinyl)-1H-indole Hydrochloride | HCID 10203482 | — |
Reaktionsschritte
The title compound was prepared from 4-(4-boc-piperazinyl)-indole and 3,4-dimethoxyphenylsulfonyl chloride according to Method 3: 1H NMR (270 MHz, DMSO-d6) δ 9.00 (br, 1 H), 7.82 (d, J=5 Hz, 1 H), 7.66 (d, J=8 Hz, 1 H), 7.57 (m, 1 H), 7.40 (d, J=3 Hz, 1 H), 7.24 (t, J=8 Hz, 1 H), 7.10 (d, J=8 Hz, 1 H), 6.90 (d, J=5 Hz, 1 H), 6.78 (d, J=8 Hz, 1 H), 3.78 (s, 6 H), 3.24 (m, 8 H); MS (ESI+) for m/z 402 (M+H)+.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07087750B2 |
| Quelldatensatz | uspto-grants-2006_08 |
| ORD ID | ord-ac0698e88e6c456cbcd88503e97c7bdc |
| Quellennotiz | uspto-grants-2006_08 |