HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Benzaldehyde → 1-Cyclohexyl-4-dimethylamino-2-phenyl-2-buten-1-ol
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Benzaldehyde | HCID 240 | — |
| Edukt | beta-Diethylaminopropiophenone 2,4,6-triisopropylbenzenesulphonylhydrazone | HCID 86741730 | — |
| Produkt | 1-Cyclohexyl-4-dimethylamino-2-phenyl-2-buten-1-ol | HCID 53845847 | — |
Reaktionsschritte
By using a method similar to that described in Example 22, but starting from β-diethylaminopropiophenone 2,4,6-triisopropylbenzenesulphonylhydrazone (30 g) and benzaldehyde (6.9 cc), 4-diethylamino-1,2-diphenyl-2-buten-1-ol (Z) hydrochloride (3.2 g) is obtained, after recrystallisation from acetone, in the form of white crystals melting at 140° C.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04755599 |
| Quelldatensatz | uspto-grants-1988_07 |
| ORD ID | ord-7e88a7e6b815446cb4810f2debc5f5bc |
| Quellennotiz | uspto-grants-1988_07 |