HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Hydrogen Bromide → HCID 178419246, Verbindung
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Hydrogen Bromide | HCID 260 | — |
| Edukt | (3-Mercaptopropyl)ammonium chloride | HCID 197870 | — |
| Edukt | 4-Methylimidazol-5-ylmethanolhydrochloride | HCID 3084707 | — |
| Produkt | HCID 178419246 | HCID 178419246 | — |
Reaktionsschritte
A solution of homocysteamine hydrochloride (22.0 g.) and 4-hydroxymethyl-5-methylimidazole hydrochloride (25.6 g.) in aqueous hydrobromic acid (500 ml.) was heated under reflux for one hour. Concentration under reduced pressure, followed by recrystallisation from methanol-isopropyl alcohol afforded 4-methyl-5-[(3-aminopropyl)thiomethyl]-imidazole dihydrobromide (24.5 g.), m.p. 200.5°-202.5°.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04293699 |
| Quelldatensatz | uspto-grants-1981_10 |
| ORD ID | ord-5c03afb5b75a493baa34d35232237405 |
| Quellennotiz | uspto-grants-1981_10 |