HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Sodium Sulfite → 2-(butylsulfonyl)cyclopentanone
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Sodium Sulfite | HCID 24437 | — |
| Edukt | Monoperoxyphthalic acid | HCID 75329 | — |
| Lösungsmittel | Diethyl Ether | HCID 3283 | — |
| Produkt | 2-(butylsulfonyl)cyclopentanone | HCID 289555 | — |
Reaktionsschritte
2-Buthylthiocyclopentanone (88 g) was reacted with a 30% excess solution of mono-perphthalic acid in ether at 0° C. After the reaction was completed, the excess mono-perphthalic acid was treated with sodium sulfite, and the resultant solution was washed, evaporated to remove the solvent, and then distilled, thereby giving 2-butylsulfonylcyclopentanone (78 g).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07252849B2 |
| Quelldatensatz | uspto-grants-2007_08 |
| ORD ID | ord-e82c9b732d564f92a08e72aaa22da92b |
| Quellennotiz | uspto-grants-2007_08 |