HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Butylamine → Phenyl n-butylcarbamate
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Butylamine | HCID 8007 | — |
| Edukt | Hexane | HCID 8058 | — |
| Edukt | Ethyl Acetate | HCID 8857 | — |
| Produkt | Phenyl n-butylcarbamate | HCID 97513 | 71,97% |
Reaktionsschritte
n-Butylamine (4.9 ml, 50 mmol) was used for the same reaction as in Production Example 310-1, and purification was performed by silica gel column chromatography (hexane:ethyl acetate=4:1) to obtain the title compound (8.11 g, 41.97 mmol, 71.97%) as a colorless oil.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07253286B2 |
| Quelldatensatz | uspto-grants-2007_08 |
| ORD ID | ord-51ba7a6db04e4598b99e8c14f289b527 |
| Quellennotiz | uspto-grants-2007_08 |