HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Acrolein → N-(4-Chlorobenzylidene)-4-methylthioaniline
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Acrolein | HCID 7847 | — |
| Edukt | alpha-(4-Chlorophenyl)-alpha-(4-methylthioanilino)acetonitrile | HCID 21862778 | — |
| Produkt | N-(4-Chlorobenzylidene)-4-methylthioaniline | HCID 21862850 | — |
Reaktionsschritte
Following a procedure similar to that described in Example 21(iii), but using α-(4-chlorophenyl)-α-(4-methylthioanilino)acetonitrile [prepared as described in step (ii) above] and acrolein as starting materials, the title compound was obtained as an orange-colored powder (yield 32%), melting at 203-205° C.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | USRE039420E1 |
| Quelldatensatz | uspto-grants-2006_12 |
| ORD ID | ord-e8566af10da04d4cb67722f52d006b8e |
| Quellennotiz | uspto-grants-2006_12 |