HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Hydrochloric Acid → 2-(1h-Pyrazol-3-yl)-benzylamine hydrochloride salt
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Hydrochloric Acid | HCID 313 | — |
| Edukt | HCID 178453037 | HCID 178453037 | — |
| Lösungsmittel | Ethyl Acetate | HCID 8857 | — |
| Produkt | 2-(1h-Pyrazol-3-yl)-benzylamine hydrochloride salt | HCID 178479178 | — |
Reaktionsschritte
Hydrogen chloride gas was bubbled through a 0° C. solution of tert-butyl 2-(1H-pyrazol-3-yl)benzylcarbamate (60 mg, 0.220 mmol) in ethyl acetate (5 ml) for 2 min and stirred for 40 min. A precipitate formed, and the suspension was concentrated in vacuo to give 2-(1H-pyrazol-3-yl)-benzylamine hydrochloride salt; MS (ES+) M+1 174.1 for C10H11N3.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07144899B2 |
| Quelldatensatz | uspto-grants-2006_12 |
| ORD ID | ord-22a5083e6e1a44fdb08b7e75ca87b653 |
| Quellennotiz | uspto-grants-2006_12 |