HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
p-Methoxybenzophenonoxime → 1-(4-Methoxyphenyl)-1-phenylmethanamine
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | p-Methoxybenzophenonoxime | HCID 185567 | — |
| Edukt | Ammonium Acetate | HCID 517165 | — |
| Edukt | Sodium cyanoborohydride | HCID 5003444 | — |
| Katalysator | titanium(III) trichloride | HCID 10313229 | — |
| Produkt | 1-(4-Methoxyphenyl)-1-phenylmethanamine | HCID 350041 | 76,9% |
Reaktionsschritte
Following a procedure similar to that described in Preparation 12, but using 9.4 g of 4-methoxybenzophenone oxime, 33.9 g of ammonium acetate, 7.46 g of sodium cyanoborohydride, and 79 ml of a 17-19% by volume aqueous solution of titanium trichloride, 6.78 g of the title compound were obtained as an oily substance.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05717088 |
| Quelldatensatz | uspto-grants-1998_02 |
| ORD ID | ord-4261112265e44ee085ca2bfb69a10958 |
| Quellennotiz | uspto-grants-1998_02 |