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HRID 863221Erstellt: 24. Oktober 2026
Butylamine → 3(R,S)-butylaminocarbonyl-1,2,3,4-tetrahydroquinoline
https://huagongshe.com/de/reaction/863221
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|
| Edukt | Butylamine | HCID 8007 | — |
| Edukt | Methyl 1,2,3,4-tetrahydro-3-quinolinecarboxylate | HCID 283526 | — |
| Produkt | 3(R,S)-butylaminocarbonyl-1,2,3,4-tetrahydroquinoline | HCID 19697883 | — |
Reaktionsschritte
A mixture of 500 mg of 3(R,S)-methoxycarbonyl-1,2,3,4-tetrahydroquinoline (Example 1r) and 1 ml of n-butylamine is stirred at 60° C. for 1 h. Purification of the crude product by means of FC over 50 g of silica gel (mobile phase Z) gives 3(R,S)-butylaminocarbonyl-1,2,3,4-tetrahydroquinoline: Rf (Z)=0.21.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patentnummer | US05719141 |
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| Quelldatensatz | uspto-grants-1998_02 |
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| ORD ID | ord-a3f062c980fa403cad2cdac12411e63c |
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| Quellennotiz | uspto-grants-1998_02 |
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