HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Ethanol → Ethyl 2-(3-hydroxy-4-methoxyphenyl)acetate
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Ethanol | HCID 702 | — |
| Edukt | Sulfuric Acid | HCID 1118 | — |
| Edukt | 3-Hydroxy-4-methoxybenzeneacetic acid | HCID 160562 | — |
| Produkt | Ethyl 2-(3-hydroxy-4-methoxyphenyl)acetate | HCID 5324706 | — |
Reaktionsschritte
To 3-hydroxy-4-methoxyphenylacetic acid (5.0 g, 23.8 mmol) in EtOH (100 mL) was added sulfuric acid (1 mL), and the reaction was stirred overnight at room temperature. Once no starting material was seen by analytical tlc, the mixture was concentrated to give the desired product.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US08242145B2 |
| Quelldatensatz | uspto-grants-2012_08 |
| ORD ID | ord-8e44c9051365405ca7c7ab4f06655442 |
| Quellennotiz | uspto-grants-2012_08 |