HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Isobutylene → N-(4-ethylphenyl)maleimide isobutene
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Isobutylene | HCID 8255 | — |
| Edukt | N-(4-Ethylphenyl)maleimide | HCID 522624 | — |
| Edukt | Neodecanoate | HCID 21225528 | — |
| Lösungsmittel | Toluene | HCID 1140 | — |
| Produkt | N-(4-ethylphenyl)maleimide isobutene | HCID 69501763 | — |
Reaktionsschritte
In a one-liter autoclave were charged 400 ml of toluene as a polymerization solvent, 0.001 moles of perbutyl neodecanoate as a polymerization initiator, 0.42 moles of N-(4-ethylphenyl)maleimide, and 4.05 moles of isobutene, and the mixture was subjected to polymerization reaction under a polymerization condition at a polymerization temperature of 60° C. for a polymerization time of 5 hours, to obtain N-(4-ethylphenyl)maleimide-isobutene alternating copolymer. The thus obtained N-(4-ethylphenyl)maleimide-isobutene alternating copolymer had a weight average molecular weight (Mw) (as reduced into standard polystyrene) of 155,000 and an Mw/Mn of 2.6.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07001967B2 |
| Quelldatensatz | uspto-grants-2006_02 |
| ORD ID | ord-5c0a5748989048e88fb11a8d59533928 |
| Quellennotiz | uspto-grants-2006_02 |