HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
1-Cyano-2-ethoxy-2-methylaminoethylene → HCID 178483853, Verbindung
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 1-Cyano-2-ethoxy-2-methylaminoethylene | HCID 73683202 | — |
| Edukt | HCID 178433288 | HCID 178433288 | — |
| Lösungsmittel | Pyridine | HCID 1049 | — |
| Produkt | HCID 178483853 | HCID 178483853 | — |
Reaktionsschritte
4-Methyl-5-[(2-aminoethyl)thiomethyl]imidazole (3.5 g) was added to a solution of 1-cyano-2-ethoxy-2-methylaminoethylene in pyridine (3.1 g) and the solution was stirred for 5 hours at 100°. The product was chromatographed on a column of neutral alumina with elution by chloroform/ethyl acetate (1:1) to give the title compound as a glass.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04284640 |
| Quelldatensatz | uspto-grants-1981_08 |
| ORD ID | ord-50434325540842ad8efa31b7e0e23544 |
| Quellennotiz | uspto-grants-1981_08 |