Zurück
HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 904770Erstellt: 24. Oktober 2026

Ammonia → (2-Nitrophenyl)methanesulfonamide

https://huagongshe.com/de/reaction/904770

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktAmmoniaHCID 222—
Edukt(2-nitrophenyl)methanesulfonyl ChlorideHCID 4305447—
LösungsmittelDiethyl EtherHCID 3283—
Produkt(2-Nitrophenyl)methanesulfonamideHCID 13266249—

Reaktionsschritte

To a suspension of 29.4 g of the product of Example 2 in 250 ml of diethyl ether was added 6.5 ml of anhydrous ammonia at 5°-15°. After stirring at 15°-25° for 1 hour, the product was filtered off, washed with ether, and water and oven dried at 60° to give 20.5 g of 2-nitrophenylmethanesulfonamide, m.p.=134°-136°.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS04420325
Quelldatensatzuspto-grants-1983_12
ORD IDord-0962ea6a32954304a1470f3d92c29e71
Quellennotizuspto-grants-1983_12