HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Chlorodiisopropylphosphine → HCID 178425660, Verbindung
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Chlorodiisopropylphosphine | HCID 538967 | — |
| Edukt | Butyllithium | HCID 178418339 | — |
| Edukt | HCID 178425630 | HCID 178425630 | — |
| Produkt | HCID 178425660 | HCID 178425660 | — |
Reaktionsschritte
Procedure as described for NP Amidine I using the following amounts: 1.19 g of 4-methyl-N1-(2,6-dimethylphenyl)benzamidine (Amidine III, 5.0 mmol), 2.50 mL of 2.0 M butyllithium (5.0 mmol), 0.80 mL chlorodiisopropylphosphine (5.0 mmol). After filtration to remove lithium chloride and removal of solvent, a yellow oil was isolated (1.76 g).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US09283555B2 |
| Quelldatensatz | uspto-grants-2016_03 |
| ORD ID | ord-7e05587c55fe4a859af7cc6655129a71 |
| Quellennotiz | uspto-grants-2016_03 |