HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Thionyl Chloride → 4-[(2-methylbenzoyl)amino]benzoyl Chloride
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Thionyl Chloride | HCID 24386 | — |
| Edukt | 4-[(2-methylbenzoyl)amino]benzoic Acid | HCID 11615814 | — |
| Produkt | 4-[(2-methylbenzoyl)amino]benzoyl Chloride | HCID 10707441 | — |
Reaktionsschritte
A mixture of 10.3 g of 4-[(2-methylbenzoyl)amino]benzoic acid and 32 ml of thionyl chloride is refluxed for 1.5 hours. The solution is concentrated under vacuum. Toluene is added and the solvent removed under vacuum. Toluene is added and the mixture chilled and filtered to give a yellow solid, m.p. 135°-141° C.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05760031 |
| Quelldatensatz | uspto-grants-1998_06 |
| ORD ID | ord-08ae3b3eba87448aaa096c664dfd605e |
| Quellennotiz | uspto-grants-1998_06 |