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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 978595Erstellt: 24. Oktober 2026

HCID 14075472, Verbindung → N,N-Diethyl-3-pyrrolidinemethanamine

https://huagongshe.com/de/reaction/978595

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktHCID 14075472HCID 14075472—
EduktHCID 178418361HCID 178418361—
KatalysatorPalladiumHCID 23938—
LösungsmittelMethanolHCID 887—
ProduktN,N-Diethyl-3-pyrrolidinemethanamineHCID 14075474101,7%

Reaktionsschritte

A mixture of 25.4 g (0.10 mole) of N,N-diethyl-1-(phenylmethyl)-3-pyrrolidinemethanamine, 200 ml of methyl alcohol, 2 g of palladium on carbon and hydrogen were shaken at a pressure of 51.5 psi. After 20.3 hours, the catalyst was filtered and the filtrate concentrated under reduced pressure. The residue was bulb to bulb distilled giving 15.9 g of N,N-diethyl-3-pyrrolidinemethanamine.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS04665079
Quelldatensatzuspto-grants-1987_05
ORD IDord-e7febe3b43c34959b96b8427691a395a
Quellennotizuspto-grants-1987_05