HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HCID 14075472, Verbindung → N,N-Diethyl-3-pyrrolidinemethanamine
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | HCID 14075472 | HCID 14075472 | — |
| Edukt | HCID 178418361 | HCID 178418361 | — |
| Katalysator | Palladium | HCID 23938 | — |
| Lösungsmittel | Methanol | HCID 887 | — |
| Produkt | N,N-Diethyl-3-pyrrolidinemethanamine | HCID 14075474 | 101,7% |
Reaktionsschritte
A mixture of 25.4 g (0.10 mole) of N,N-diethyl-1-(phenylmethyl)-3-pyrrolidinemethanamine, 200 ml of methyl alcohol, 2 g of palladium on carbon and hydrogen were shaken at a pressure of 51.5 psi. After 20.3 hours, the catalyst was filtered and the filtrate concentrated under reduced pressure. The residue was bulb to bulb distilled giving 15.9 g of N,N-diethyl-3-pyrrolidinemethanamine.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04665079 |
| Quelldatensatz | uspto-grants-1987_05 |
| ORD ID | ord-e7febe3b43c34959b96b8427691a395a |
| Quellennotiz | uspto-grants-1987_05 |