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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 979694Erstellt: 23. Oktober 2026

Silane, ethenyltris(1-methylethoxy)- → 1-Tritertbutoxysilyl-2-triisopropoxysilylethylene

https://huagongshe.com/de/reaction/979694

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktSilane, ethenyltris(1-methylethoxy)-HCID 87409—
EduktTris(tert-butoxy)silaneHCID 101075511—
LösungsmittelO-XyleneHCID 7237—
Produkt1-Tritertbutoxysilyl-2-triisopropoxysilylethyleneHCID 54208286—

Reaktionsbedingungen

Temperatur225 °C

Reaktionsschritte

Into a 45 cc Parr bomb was added 2.5 g (0.010 mol) tritertbutoxysilane, 4.7 g (0.020 mol) vinyltriisopropoxysilane, 1.0 g xylene and 2000 ppm Ru3CO12 (29 mg) as a catalyst. The reaction was heated to 225° C. for 3 hours in a fluidized sand bath. A single product, 1-tritertbutoxysilyl-2-triisopropoxysilylethylene was formed.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS04668812
Quelldatensatzuspto-grants-1987_05
ORD IDord-ce0c828dc6334923bb02036296c792c4
Quellennotizuspto-grants-1987_05