HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Boron, trifluoro(methanol)-, (T-4)- → Methyl 2-(3-methoxyphenyl)-5-oxo-1-phenylpyrrolidin-3-carboxylate
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Boron, trifluoro(methanol)-, (T-4)- | HCID 11062313 | — |
| Edukt | 2-(3-Methoxyphenyl)-5-oxo-1-phenylpyrrolidin-3-carboxylic acid | HCID 13361985 | — |
| Produkt | Methyl 2-(3-methoxyphenyl)-5-oxo-1-phenylpyrrolidin-3-carboxylate | HCID 13362002 | — |
Reaktionsschritte
A solution of 25.0 gm. of 2-(3-methoxyphenyl)-5-oxo-1-phenylpyrrolidin-3-carboxylic acid in 200 ml 10-15% boron fluoride-methanol was refluxed for 8 hours and upon following the workup for example 1C the product was obtained as an oil.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04639529 |
| Quelldatensatz | uspto-grants-1987_01 |
| ORD ID | ord-547bbf377ac84c26a22b0895622c04ce |
| Quellennotiz | uspto-grants-1987_01 |