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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 981010Erstellt: 24. Oktober 2026

8(5H)-Quinolinone, 5-[[4-(diethylamino)-2-methylphenyl]imino]-, (5Z)- → Indoaniline

https://huagongshe.com/de/reaction/981010

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
Edukt8(5H)-Quinolinone, 5-[[4-(diethylamino)-2-methylphenyl]imino]-, (5Z)-HCID 364894—
LösungsmittelEthanolHCID 702—
LösungsmittelWaterHCID 962—
ProduktIndoanilineHCID 24748760—

Reaktionsschritte

Then, a solution prepared by dissolving 285.3 mg of Ni(ClO4)2.6H2O in 50 ml of water, was added under a nitrogen atmosphere to a solution prepared by dissolving 100 mg of 5-(2'-methyl-4'-diethylaminophenylimino)quinoline-8-one obtained above in 50 ml of 99% ethanol, and the mixture was stirred at room temperature for about 30 minutes. Formed precipitates were subjected to suction filtration, washed with water and dried to obtain a metal-containing indoaniline compound having the formula: ##STR9##

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS04990433
Quelldatensatzuspto-grants-1991_02
ORD IDord-d8d61d8ff3454d6b8cbc42e442683859
Quellennotizuspto-grants-1991_02