HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
3,4-Dichloroaniline → Ethyl N-(3,4-dichlorophenyl)alaninate
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 3,4-Dichloroaniline | HCID 7257 | — |
| Edukt | Ethyl pyruvate | HCID 12041 | — |
| Produkt | Ethyl N-(3,4-dichlorophenyl)alaninate | HCID 169545 | — |
Reaktionsschritte
Following General Procedure AA above and using 3,4-dichloroaniline (Aldrich) and ethyl pyruvate (Aldrich), the title compound was prepared as an oil. The reaction was monitored by tlc on silica gel (Rf=0.4 in 25% EtOAc/hexanes) and purification was by preparative plate chromatography (silica gel using 25% EtOAc/hexanes as the eluant).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US06635632B1 |
| Quelldatensatz | uspto-grants-2003_10 |
| ORD ID | ord-3cec600142bf495591ff47524e28c971 |
| Quellennotiz | uspto-grants-2003_10 |