HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
(4-Hydroxyphenyl)diphenylsulfonium chloride → (p-Hydroxyphenyl)diphenylsulfonium trifluoromethanesulfonate
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | (4-Hydroxyphenyl)diphenylsulfonium chloride | HCID 18411308 | — |
| Edukt | Potassium Trifluoromethanesulfonate | HCID 23664779 | — |
| Produkt | (p-Hydroxyphenyl)diphenylsulfonium trifluoromethanesulfonate | HCID 22389942 | — |
Reaktionsschritte
To an aqueous solution of 11.5 g of the diphenyl-4-hydroxyphenylsulfonium chloride, 22 g of an aqueous 37.5% potassium trifluoromethanesulfonate solution was dropwise added with stirring at room temperature to obtain a white precipitate. The white precipitate was filtered, and then the impurities were washed with distilled water several times, followed by drying under reduced pressure to obtain 10.7 g of the desired diphenyl-4-hydroxyphenylsulfonium trifluoromethanesulfonate.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US06468714B2 |
| Quelldatensatz | uspto-grants-2002_10 |
| ORD ID | ord-687c6ba1df6a4c13b38b4937adaba582 |
| Quellennotiz | uspto-grants-2002_10 |