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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1015Generated: October 23, 2026

4-Chloro-3-methoxy-2-methylpyridine → 4-(3,3-Dimethyl-1,5-dioxaspiro[5.5]undecan-9-yloxy)-3-methoxy-2-methylpyridine

https://huagongshe.com/en/reaction/1015

Reaction equation

Participants

RoleNameHCIDCharge
Reactant4-Chloro-3-methoxy-2-methylpyridineHCID 10583046—
Reactant3,3-Dimethyl-1,5-dioxaspiro[5.5]undecan-9-olHCID 12470096—
Product4-(3,3-Dimethyl-1,5-dioxaspiro[5.5]undecan-9-yloxy)-3-methoxy-2-methylpyridineHCID 1969393475%

Reaction Steps

Preparation was carried out analogously to Example 43 from 4-chloro-3-methoxy-2-methylpyridine and 3,3-dimethyl-1,5-dioxaspiro[5.5]undecan-9-ol. Yield: 75%; M.p.: 90° C.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05723450
Source datasetuspto-grants-1998_03
ORD IDord-23dc3d980fa24e5c82e553d717c3da9c
Source noteuspto-grants-1998_03