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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1163913Generated: October 24, 2026

N,N-Diphenylhydrazine → N-Ethylcarbazole-3-carbaldehyde diphenylhydrazone

https://huagongshe.com/en/reaction/1163913

Reaction equation

Participants

RoleNameHCIDCharge
ReactantN,N-DiphenylhydrazineHCID 10739—
Reactant9-ethyl-9H-carbazole-3-carbaldehydeHCID 82055—
SolventEthanolHCID 702—
ProductN-Ethylcarbazole-3-carbaldehyde diphenylhydrazoneHCID 175429—

Reaction Steps

1,1-diphenylhydrazine and N-ethylcarbazole-3-carbaldehyde were reacted in ethanol at room temperature to obtain N-ethylcarbazole-3-carbaldehyde diphenylhydrazone with melting point of 160.2°-160.5° C., and 60 parts of this hydrazone compound and 100 parts of a polyester (Vylon 200 by Toyobo Co., Ltd.) were dissolved in 450 parts of tetrahydrofuran to prepare a coating solution. Then selenium was vacuum evaporated on a 10 μm thick aluminum foil laminated on a 75 μm thick polyester film to form a charge generating layer with thickness of approximately 0.3 μm, and to this layer was applied the above-said coating solution by a film applicator and dried to form a 20 μm thick charge transporting layer. In this way, there was obtained a double-layer type electrophotographic plate.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04367273
Source datasetuspto-grants-1983_01
ORD IDord-eef9d805676f44cc89f89adc154effdf
Source noteuspto-grants-1983_01