HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl 2-butyryl-3-ethoxyacrylate → HCID 178450502, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl 2-butyryl-3-ethoxyacrylate | HCID 3359484 | — |
| Reactant | 5-Ethoxy-6-methylpyridin-2-amine | HCID 12875017 | — |
| Product | HCID 178450502 | HCID 178450502 | — |
Reaction Steps
Ethyl 2-(ethoxymethylene)-3-oxohexanoate (22.4 g) was added to a suspension of 5-ethoxy-6-methylpyridin-2-amine (14.9 g) in IMS (50 ml). After the initial exotherm had subsided IMS (100 ml) was added and the mixture boiled under reflux until a solution was obtained. This solution was cooled and filtered to give ethyl 2-(5-ethoxy-6-methylpyrid-2-ylaminomethylene)-3-oxohexanoate, m.p. 117°-120° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05464781 |
| Source dataset | uspto-grants-1995_11 |
| ORD ID | ord-bfd9709289484cfd9994972d7ffdb45d |
| Source note | uspto-grants-1995_11 |