HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Iodide → 4-Iodo-5h-dibenzo[a, d]cyclohepten-5-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Iodide | HCID 4875 | — |
| Reactant | 5H-Dibenzo[a,d]cyclohepten-5-one | HCID 16679 | — |
| Reactant | Thallium(1+);2,2,2-trifluoroacetate | HCID 21902506 | — |
| Product | 4-Iodo-5h-dibenzo[a, d]cyclohepten-5-one | HCID 58646849 | — |
Reaction Steps
2.06 g of dibenzosuberenone [CAS No. 2222-33-5] was subjected to the procedure of Example 1-g using 6.5 g of thallium trifluoroacetate and 2.0 g of potassium iodide, to give 1.0 g of a mixture of the title compound with dibenzosuberenone as a colorless powder.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07390797B2 |
| Source dataset | uspto-grants-2008_06 |
| ORD ID | ord-8c5115ce7ec94e08aca40e7dc434c12b |
| Source note | uspto-grants-2008_06 |