HuagongsheHuagongshe Chemistry Print Report · For research reference only
6-Aminohexanoic Acid → HCID 178512818, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 6-Aminohexanoic Acid | HCID 564 | — |
| Reactant | Sodium Carbonate | HCID 10340 | — |
| Reactant | Methanesulfonic acid, aminoimino- | HCID 9877361 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 178512818 | HCID 178512818 | — |
Reaction Steps
6.5 g (50 mmol) 6-aminohexanoic acid and 6.9 g (50 mmol) sodium carbonate were dissolved in 50 mL water. 6.2 g (50 mmol) amino-iminomethane sulphonic acid was added under stirring to the solution. After 20 hours, the product was filtered and washed with acetic acid, methanol and then ether. Yield: 6.6 g (76%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07732378B2 |
| Source dataset | uspto-grants-2010_06 |
| ORD ID | ord-5a319964270d42289d6889c6bc678cfb |
| Source note | uspto-grants-2010_06 |