3-Amino-4-methoxybenzanilide → HCID 53919419, compound

HRID 1859714

Reaction equation

HRID 1859714 reaction equation
[NH2:1][C:2]1[CH:3]=[C:4]([CH:14]=[CH:15][C:16]=1[O:17][CH3:18])[C:5]([NH:7][C:8]1[CH:13]=[CH:12][CH:11]=[CH:10][CH:9]=1)=[O:6].[CH3:19][C:20]1[CH:21]=[C:22]([N:27]=[C:28]=[S:29])[CH:23]=[C:24]([CH3:26])[CH:25]=1>>[CH3:19][C:20]1[CH:21]=[C:22]([NH:27][C:28](=[S:29])[NH:1][C:2]2[CH:3]=[C:4]([CH:14]=[CH:15][C:16]=2[O:17][CH3:18])[C:5]([NH:7][C:8]2[CH:13]=[CH:12][CH:11]=[CH:10][CH:9]=2)=[O:6])[CH:23]=[C:24]([CH3:26])[CH:25]=1

Participants

3

Reactant 2

HCID 84263-Amino-4-methoxybenzanilideHCID 1424063,5-Dimethylphenyl Isothiocyanate

Product 1

HCID 53919419HCID 53919419, compoundYield 25.8%

Procedure

Prepared according to the procedure described for Example 98 using 3-amino-4-methoxy-N-phenyl-benzamide (0.974 g, 4.01 mmol) and 3,5-dimethylphenyl isothiocyanate (0.66 g, 4.04 mmol) to afford the product (0.42 g); m.p. 203-205° C.

Workup

  1. customPrepared

Sources & evidence

ORD record
ord-8eb5b1e300014645bc54786c85e72cd0
Source dataset
uspto-grants-2003_03
Patent number
US06528528B2

Linked notes

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