HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Amino-6-methylpyridine → (5-Methyl-2-phenanthren-9-yl-imidazo[1,2-a]pyridin-3-yl)-(1,1,3,3-tetramethylbutyl)-amine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Amino-6-methylpyridine | HCID 15765 | — |
| Reactant | 1,1,3,3-Tetramethylbutyl isocyanide | HCID 26725 | — |
| Reactant | Phenanthrene-9-carbaldehyde | HCID 78437 | — |
| Solvent | Perchloric Acid | HCID 24247 | — |
| Product | (5-Methyl-2-phenanthren-9-yl-imidazo[1,2-a]pyridin-3-yl)-(1,1,3,3-tetramethylbutyl)-amine | HCID 22591923 | — |
Reaction Steps
Compound (36) was prepared according to the general synthesis instructions from 1.0 ml of 2-amino-6-methylpyridine solution (0.1 M, DCM), 0.575 ml of 1,1,3,3-tetramethylbutyl isocyanide solution (0.2 M, DCM), 0.500 ml of phenanthrene-9-carbaldehyde solution (0.3 M, DCM), and 10 μl of perchloric acid (w=20%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06849642B2 |
| Source dataset | uspto-grants-2005_02 |
| ORD ID | ord-dfda71c95a32446db74fee15f2c8a064 |
| Source note | uspto-grants-2005_02 |