4-Aminobenzoic Acid → p-((1-Oxoallyl)amino)benzoic acid

HRID 2380691

Reaction equation

HRID 2380691 reaction equation
[NH2:1][C:2]1[CH:10]=[CH:9][C:5]([C:6]([OH:8])=[O:7])=[CH:4][CH:3]=1.[C:11](Cl)(=[O:14])[CH:12]=[CH2:13]>>[C:11]([NH:1][C:2]1[CH:10]=[CH:9][C:5]([C:6]([OH:8])=[O:7])=[CH:4][CH:3]=1)(=[O:14])[CH:12]=[CH2:13]

Participants

3

Reactant 2

HCID 9784-Aminobenzoic AcidHCID 13140Acryloyl chloride

Product 1

HCID 84866p-((1-Oxoallyl)amino)benzoic acid

Procedure

The monomer was prepared from p-aminobenzoic acid reaction with acryloyl chloride, per Example 1. The monomer was recrystallized from an ethanol-water mixture and dried to produce a crystalline solid with a melting point of 249°-253° C.

Workup

  1. customThe monomer was recrystallized from an ethanol-water mixture
  2. customdried
  3. customto produce a crystalline solid with a melting point of 249°-253° C.

Sources & evidence

ORD record
ord-3c8d4cb4e8ef40be8625e4f8bf69a6c1
Source dataset
uspto-grants-1994_11
Patent number
US05369142

Linked notes

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