HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Bromohexane → Methyl 5-n-hexyloxy-2-hydroxybenzoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Bromohexane | HCID 8101 | — |
| Reactant | Methyl Gentisate | HCID 75077 | — |
| Product | Methyl 5-n-hexyloxy-2-hydroxybenzoate | HCID 19036686 | 58% |
Reaction Steps
Synthesis was carried out in the same manner as in Example 1, except for replacing methyl 2,4-dihydroxybenzoate with methyl 2,5-dihydroxybenzoate and replacing 2-ethylhexyl bromide with n-hexyl bromide, to obtain methyl 5-n-hexyloxy-2-hydroxybenzoate represented by the following chemical formula (hereinafter referred to as compound 12) as a colorless, clear and oily substance in a yield of 58%. The analytical results are shown below. ##STR33##
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05646184 |
| Source dataset | uspto-grants-1997_07 |
| ORD ID | ord-067a1c54dc8644329a2034184a965103 |
| Source note | uspto-grants-1997_07 |