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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 362740Generated: October 23, 2026

Glycerol → Diethylene Glycol Monobutyl Ether

https://huagongshe.com/en/reaction/362740

Reaction equation

Participants

RoleNameHCIDCharge
ReactantGlycerolHCID 753—
ReactantRhodamine BHCID 6694—
ReactantDiethylene GlycolHCID 8117—
SolventWaterHCID 962—
ProductDiethylene Glycol Monobutyl EtherHCID 8177—
Product3,5-Dimethyl-1-hexyn-3-olHCID 61018—

Reaction Steps

A solution containing 2.50 g Kayacryl Rhodamine FB (Product Name, Nippon Kayaku, C.I. Acid Red 52), 0.06 g LM pectin (Product Name: LM-104AS, The Copenhagen Pectin Factory Ltd.), 5.00 g of glycerol, 5.00 g of diethylene glycol, 8.00 g diethylene glycol mono-n-butyl ether, 0.80 g of Surfynol 465, and 78.64 g of ultrapure water was prepared. The solution was stirred for 2 hours and then filtered through a 5 μm stainless steel mesh.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05871572
Source datasetuspto-grants-1999_02
ORD IDord-f327446fd5674b8fbf64d4cfd9b29b4d
Source noteuspto-grants-1999_02