HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzoic Acid → 1,1,1,3,3,3-Hexafluoropropane
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzoic Acid | HCID 243 | — |
| Reactant | bisphenol AF | HCID 73864 | — |
| Product | 1,1,1,3,3,3-Hexafluoropropane | HCID 12722 | 89% |
Reaction Steps
A reaction was conducted as described in Example 6 except that benzoic acid was replaced with 105 mmol of 2,2-bis(4-hydroxyphenyl)-1,1,1,3,3,3-hexafluoropropane and the amount of PGE was 200 mmol. Desired 2,2-bis[4-(2-hydroxy-3-phenoxypropyloxy)phenyl[-1,1,1,3,3,3-hexafluoropropane was formed in analytical yield of 89% and isolated in a yield of 83%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06130346 |
| Source dataset | uspto-grants-2000_10 |
| ORD ID | ord-91ba050f309d4a999d59440f4a716774 |
| Source note | uspto-grants-2000_10 |