HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzyl Alcohol → o-Phenylphenol 2-methyl-4-isothiazolinone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzyl Alcohol | HCID 244 | — |
| Reactant | (1,1'-Biphenyl)-2-ol | HCID 7017 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | Methylisothiazolinone | HCID 39800 | — |
| Solvent | Water | HCID 962 | — |
| Product | o-Phenylphenol 2-methyl-4-isothiazolinone | HCID 86758987 | — |
Reaction Steps
A solution of o-phenylphenol/2-methyl-4-isothiazolinone was prepared by dissolving 25 g of o-phenylphenol and 12.5 g 2-methyl-4-isothiazolinone using 20 g monopropylene glycol and 20 g benzyl alcohol and 2.5 g NaOH and 20 g water to achieve a 25% by wt. solution, based on o-phenylphenol and a 12.5% solution, based on MIT.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06569229B1 |
| Source dataset | uspto-grants-2003_05 |
| ORD ID | ord-ee060bf050984e91a25284deabd7f75a |
| Source note | uspto-grants-2003_05 |