2-(Cyclohexylthio)-1H-isoindole-1,3(2H)-dione → HCID 88807735, compound

HRID 435730

Reaction equation

HRID 435730 reaction equation
[C:1]([OH:4])(=[S:3])[CH3:2].[CH:5]1([S:11]N2C(=O)C3=CC=CC=C3C2=O)[CH2:10][CH2:9][CH2:8][CH2:7][CH2:6]1>C1C=CC=CC=1>[C:1]([S:3][S:11][CH:5]1[CH2:10][CH2:9][CH2:8][CH2:7][CH2:6]1)(=[O:4])[CH3:2]

Participants

4

Reactant 2

HCID 287772-(Cyclohexylthio)-1H-isoindole-1,3(2H)-dioneHCID 178418634HCID 178418634, compound

Product 1

HCID 88807735HCID 88807735, compoundYield 98%

Reagents, catalysts & solvents 1

HCID 241BenzeneSolvent

Procedure

Thioacetic acid, 0.044 moles, 3.35 grams, is reacted with N-(cyclohexylthio)phthalimide in 100 ml of benzene and the product recovered following a procedure similar to Example 11. Acetylcyclohexyl disulfide, an amber oil, is recovered in 98% yield (7.5 grams). Analysis gives 51.27%C, 7.41%H and 31.78%S compared to 50.6%C, 7.38%H and 33.7%S calculated for C8H14OS2.

Workup

  1. customthe product recovered
  2. customAcetylcyclohexyl disulfide, an amber oil, is recovered in 98% yield (7.5 grams)
  3. customAnalysis gives 51.27%C, 7.41%H and 31.78%S

Sources & evidence

ORD record
ord-c03ecf6c99684936b0abe146aa4e1bb9
Source dataset
uspto-grants-1977_02
Patent number
US04006155

Linked notes

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