HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Hydroxide → N-{8-[(1,3-benzodioxol-5-ylcarbonyl)amino]octyl}-1,3-benzodioxole-5-carboxamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Reactant | 1,8-Octanediamine | HCID 24250 | — |
| Reactant | 1,3-Benzodioxole-5-carbonyl chloride | HCID 2734749 | — |
| Solvent | 1,2-Dichloroethane | HCID 11 | — |
| Product | N-{8-[(1,3-benzodioxol-5-ylcarbonyl)amino]octyl}-1,3-benzodioxole-5-carboxamide | HCID 3542149 | — |
Reaction Steps
m.p. 179°-180° C., 21.6 g., was prepared as in Example 1 using 3,4-methylenedioxybenzoyl chloride (from 30 g. of 3,4-methylenedioxybenzoic acid as in Example 6) in 100 ml. of ethylene dichloride, 11.5 g. of 1,8-octanediamine, 200 ml. of 10% aqueous potassium hydroxide solution, 500 ml. of ethylene dichloride and recrystallization from ethanol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04009208 |
| Source dataset | uspto-grants-1977_02 |
| ORD ID | ord-ba41fc3b76a24b8986fac562f02932ee |
| Source note | uspto-grants-1977_02 |