HuagongsheHuagongshe Chemistry Print Report · For research reference only
4,4'-Dimethoxydiphenylamine → HCID 22263989, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4,4'-Dimethoxydiphenylamine | HCID 7571 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | Sodium Cyanate | HCID 517096 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 22263989 | HCID 22263989 | — |
Reaction Steps
A solution of 423 mg (1.85 mmol) bis-(4-methoxy-phenyl)-amine in 8 ml acetic acid is treated with 120 mg (1.85 mmol)sodium cyanate. After 4.5 h the reaction mixture is poured onto a solution of 8 g sodium hydroxide in 100 ml water. The resultant precipitate is filtered off and dried.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08476286B2 |
| Source dataset | uspto-grants-2013_07 |
| ORD ID | ord-72bc243ee16e4ae2af60edf972a6d488 |
| Source note | uspto-grants-2013_07 |