HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,1,3,3-Tetrabromoacetone → HCID 68731784, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,1,3,3-Tetrabromoacetone | HCID 608441 | — |
| Reactant | Methyl 2,5-dimethyl-1H-pyrrole-1-carboxylate | HCID 12374590 | — |
| Product | HCID 68731784 | HCID 68731784 | — |
Reaction Steps
The title compound was prepared from 2,5-dimethyl-pyrrole-1-carboxylic acid methyl ester (U.S. Pat. No. 4,551,540) and 1,1,3,3-tetrabromoacetone utilizing the [4+3] cycloaddition protocol of Kim and Hoffmann (European Journal of Organic Chemistry (2000), (12), 2195-2201). Mass spectrum (ESI, m/z): Calcd. for C11H15NO3, 210.1 (M+H), found 210.0.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08497376B2 |
| Source dataset | uspto-grants-2013_07 |
| ORD ID | ord-e11c0e1c64c44dd3a084b0698fc71249 |
| Source note | uspto-grants-2013_07 |