HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrazine, [4-[(trifluoromethyl)thio]phenyl]- → HCID 58731518, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrazine, [4-[(trifluoromethyl)thio]phenyl]- | HCID 10420564 | — |
| Reactant | 5-Methyl-6-oxoheptanesulfonic acid | HCID 57903351 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 58731518 | HCID 58731518 | 14.2% |
Reaction Steps
To 4-(trifluoromethylthio)phenylhydrazine (1 g) in acetic acid (40 ml) was added 5-methyl-6-oxoheptane-1-sulphonic acid (1.4 g) and the solution heated to reflux overnight. The volatiles were removed on a rotary evaporator to give the crude product, 1.1 g of which was purified by preparative HPLC. The relevant fractions were combined, concentrated on a rotary evaporator and freeze dried to give the desired product (260 mg). M+=381
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07767829B2 |
| Source dataset | uspto-grants-2010_08 |
| ORD ID | ord-7773518b75a34179bcb983a4bc6863e6 |
| Source note | uspto-grants-2010_08 |